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    Please use this identifier to cite or link to this item: https://ir.cnu.edu.tw/handle/310902800/28073


    標題: 移動相中添加β-環糊精在逆相液相層析上分離一些單取代酚類位置異構物
    Separation of Some Isomeric Monosubstituted Phenols by RPLC Using β-cyclodextrin as Mobile Phase Additives
    作者: 李冠儀
    張書文
    賴鈺森
    林振興
    貢獻者: 輔英科技大學應用化學及材料科學系
    關鍵字: 逆相液相層析
    β-環糊精
    硝基酚
    甲酚
    乙酚
    萘酚
    Reversed Phase Liquid Chromatography
    β-Cyclodextrin
    Nitrophenol
    Cresol
    Ethylphenol
    naphthol
    日期: 2013-12
    上傳時間: 2014-10-02 16:05:57 (UTC+8)
    摘要: 本研究在移動相中添加5 mM β-環糊精於甲醇與水的混合溶液,利用RP-C18 靜相管柱分離一些單取代酚類位置異構物,並探討移動相中甲醇含量的影響。由層析結果顯示甲醇與水比例,會顯著影響單取代酚?位置?構物的分?效果。添加 5 mM β-環糊精於適當比例的甲醇與水的混合溶液當移動相,利用RP-C18 靜相管柱可以有效分離硝基酚、甲酚、乙酚以及萘酚位置異構物,且硝基酚與乙酚可以達到基線分離。
    The retention behavior of some isomeric mono-substituted phenols was investigated by high-performance liquid chromatography on a RP-C18 stationary phase using β-cyclodextrin as mobile phase additives. Effects of methanol content of mobile phase were examined. Effective separations of some isomeric mono-substituted phenols were achieved on a RP-C18 stationary phase using β-cyclodextrin as mobile phase additives. Moreover, baseline separations of isomeric nitrophenol and ethylphenol were achieved.
    關聯: 嘉南學報(科技類), n.39, pp.56-62
    Appears in Collections:[嘉南學報] 39 期 (2013)

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