Ultrasound-assisted extraction and quantitation of oils from Syzygium aromaticum flower bud (clove) with supercritical carbon dioxide

doi:10.1016/j.chroma.2013.10.098

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Title:	Ultrasound-assisted extraction and quantitation of oils from Syzygium aromaticum flower bud (clove) with supercritical carbon dioxide
Authors:	Yang, Yu-Chiao Wei, Ming-Chi Hong, Show-Jen
Contributors:	環境工程與科學系
Keywords:	Supercritical carbon dioxide extraction Ultrasound-assisted extraction Oil Syzygium aromaticum flower bud Clove Heat reflux extraction
Date:	2014-01
Issue Date:	2015-05-06 21:26:50 (UTC+8)
Publisher:	Elsevier Science Bv
Abstract:	This study evaluated ultrasound-assisted supercritical carbon dioxide (USC-CO2) extraction for determining the extraction yields of oils and the contents of eugenol, P-caryophyllene, eugenyl acetate and ot-humulene from clove buds. Compared to traditional SC-CO2 extraction, USC-CO2 extraction might provide a 13.5% increase in the extraction yield for the oil while utilizing less severe operating parameters, such as temperature, pressure, CO2 flow rate and the time consumed by the process. Our results were comparable to those obtained using the heat reflux extraction method, though the yield was improved by 20.8% using USC-CO2. In kinetic studies, the USC-CO2 extraction of clove oil followed second-order kinetics. The activation energy for the oil extraction was 76.56 kJ/mol. The USC-CO2 procedure facilitated the use of mild extraction conditions, improved extraction efficiency and the quality of products and is a potential method for industry. (C) 2013 Elsevier B.V. All rights reserved.
Relation:	Journal of Chromatography A, v.1323, pp.18-27
Appears in Collections:	[Dept. of Environmental Engineering and Science (including master's program)] Periodical Articles

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