利用氣體層析儀(Shimadzu GC-5A)採用1.5%Silicone GE-SE-30及1.5% Silicone OV-17二支2mx3mm Glass Columm，以程式升溫法對市售15種中藥風濕症治療劑加以測定分析，檢定是否含有西藥成分，以建立一可行的化驗法，並對其含量加以部分檢討，結果在15種檢品中發現了含有Aminopyrin, Phenylbutazone, Acetaminophen, Prednisolone以及Allylisopropylacetylurea 15種檢品當中6種含Aminopyrin，而最高含量高達200mg/5pills。15種檢品中9種含有Phenylbutazone，而最高含量達100mg/5pills。 A gas chromatographic method for separation and analysis of 15 samples of Chinese antirheumatic drugs by using 2mx3mm column packing 1.5% Silicone GE-SE-30 or 1.5% Silicone OV-17 in glass column with t temperature programmed chromatograph over a column temperature range 150 to 250℃.Aminopyrin, phenybutazone, Acetaminophen prednisolone, and allylisopropyl-acetylurea bad been found in 9 of samples. It was found that the maximum contents of aminopyrine was 200mg/5 pills and phenylbutazone was 100mg/5 pills.
