黃柏鹼與阿克利諾兒混合製劑之層析分析

CNU IR > Chna Nan Annual Bulletin > Vol.4 (1978) > Item 310902800/27988

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Title:	黃柏鹼與阿克利諾兒混合製劑之層析分析 Chromatographic Separation and Determination of Acrinol and Berberine in Mixed Pharmaceutical Preparations
Authors:	陳聯仕楊竹茂
Contributors:	私立嘉南藥學專科學校
Date:	1978
Issue Date:	2014-06-05 15:02:46 (UTC+8)
Abstract:	以矽膠 ( Silica gel G )為擔體，氯仿與甲醇 ( 4 : 1 )混合液為展開劑之薄層層析，於366nm螢光燈下能檢測出黃柏鹼( Berberine )與阿克利諾兒l Acrinol )之方法，簡便而迅速，效果良好。以羧基甲基纖維素 ( CM- CelJulose )為吸附劑之柱層層析，先以1 %( V/V )鹽酸溶液溶出黃柏鹼( Berberine )，再以20% ( V/V)醋酸溶液溶出阿克利諾兒( Acrinol )，於分離後，分別和標準品溶液或對照溶液，黃柏鹼( Berberine )於421 - 422 nm，阿克利諾兒於410 nm，以比色試驗作定量分析，其分離效果良好，所得結果準確，是藥廠品質管制上一理想方法。 Acrinol and berberine were detected by TLC method (silica gel, chloroform : methanol = 4:1) under UV 366 lamp against standard solution. For quantitative purpose, both ingredients were separated by column chromatographic method with CM-Cellulose column using 1% HC1 for berberine and 20% acetic acid solution were determined by colorimetric method. it gave a satisfactory results and proved to be an ideal method for the quality control of the pharmaceutial industry.
Relation:	嘉南學報, n.4 pp.23-32
Appears in Collections:	[Chna Nan Annual Bulletin] Vol.4 (1978)

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