Efficient Synthesis of 4,5-Disubstituted-3-toluenesulfonyl Glutarimides. Application to the Formal Synthesis of Mappicine Ketone

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標題:	Efficient Synthesis of 4,5-Disubstituted-3-toluenesulfonyl Glutarimides. Application to the Formal Synthesis of Mappicine Ketone
作者:	Yung-Sheng Wang Nein-Chen Chang Ching-Han Lin Huo-Mu Tai
貢獻者:	醫藥化學系
關鍵字:	Ethyl α β-disubstituted acrylate esters [3+3] Annulation Mappicine ketone
日期:	2008-04
上傳時間:	2009-10-13 09:09:28 (UTC+8)
出版者:	Chinese Chemical Soc
摘要:	Various 4,5-disubstituted-3-sulfonyl glutarimides 3 were synthesized from α-sulfonyl acetamide 1 and ethyl α,β-disubstituted acrylate esters 2 via stepwise facile [3+3] annulation in moderate yield. The synthesis of pyridin-2-one 9, a key intermediate for mappicine ketone (4) synthesis, was also reported.
關聯:	Journal of the Chinese Chemical Society 55(2)：p.431-434
显示于类别:	[食藥產業暨檢測科技系(含五專)] 期刊論文

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