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    Please use this identifier to cite or link to this item: http://ir.cnu.edu.tw/handle/310902800/25473


    標題: 以Amine-s-triazine-C18 鍵結靜相在HPLC上分離多環芳香烴
    Use of Amine-s-triazine-C18 Bonded Phase for the Separation of Polycyclic Aromatic Hydrocarbons by HPLC
    作者: 廖麗芳
    楊朝成
    張書文
    吳忠誠
    林振興
    貢獻者: 輔英科技大學應用化學及材料科學系
    嘉南藥理科技大學化粧品科技研究所
    關鍵字: 高效液相層析
    多環芳香烴
    s-三口井環
    High-PerformanceLiquidChromatography
    PolycyclicAromaticHydrocarbons
    s-Triazine
    日期: 2011-12
    上傳時間: 2012-06-08 15:10:04 (UTC+8)
    摘要: 本研究製備amine-s-triazine-C18 鍵結靜相的目的,在於分離多環芳香烴。以amine-s-triazine-C18 鍵結靜相在HPLC 上,對一些多環芳香烴的分離及滯留行為的探討。在移動相中,乙腈與水比例為55:45 時,可以有效分離7 種多環芳香烴。由層析結果顯示,鍵結靜相與分析物之間的疏水性作用力以及π-π 作用力,在滯留機轉上,扮演重要的角色。
    The amine-s-triazine-C18 bonded phase was prepared for the separation of polycyclic aromatic hydrocarbons. The separation and retention behavior of seven polycyclic aromatic hydrocarbons was investigated in HPLC using Amine-s-triazine-C18 bonded phase. Effective separations of the seven polycyclic aromatic hydrocarbons were achieved using acetonitrile-water (55:45, v/v) in mobile phase. Chromatographic results indicate that π-π interaction and hydrophobic interaction between the bonded phase and analytes play significant roles in the retention mechanism.
    關聯: 嘉南學報(科技類) 37期:p.8-13
    Appears in Collections:[嘉南學報] 37 期 (2011)
    [化妝品應用與管理系(所)] 期刊論文

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