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    Please use this identifier to cite or link to this item: http://ir.cnu.edu.tw/handle/310902800/1035


    標題: 以高效液相層析及可逆相管柱分離及純肉桂酸之順反異購物
    Separation of the racemic mixtures of cinnamic acids by HPLC with a semi-preparative C18 column
    作者: 孫芳明
    貢獻者: 保健營養系
    關鍵字: 高效液相層析
    同分異構物
    肉桂酸
    離子交換樹脂層析
    HPLC
    racemic mixtures
    cinnamic acid
    日期: 2004
    上傳時間: 2008-06-24 10:11:46 (UTC+8)
    出版者: 台南縣:嘉南藥理科技大學保健營養系
    摘要: 在此研究中我們發展出利用高效液相層析來分離肉桂酸同分異構物的方法,分離順-反式肉桂酸的高效液相層析最佳條件為:移動相甲醇與去離子水55:45(含0.5 %醋酸)、移動相流速為7.5 ml/min 、樣品注射量則為250μl。由此分離方法所純化出來的順-式肉桂酸的穩定性經測試後超過一年,此項結果建議利用高效液相層析法來分離肉桂酸同分異構物的方法比利用離子交換樹脂來分離肉桂酸同分異構物的方法更好且更準確。
    A HPLC method was developed to
    separate racemic mixtures of cinnamic
    acid in this study. The best conditions
    for the separation of trans-, and
    cis-cinnamic acids were: mobile phase
    MeOH and water : 55:45 (contains 0.5
    % acetic acid, flow rate 7.5 ml/min, and
    injection volume 250 μl. The stability
    of the cis-isomer prepared by this study
    has been shown to be more than one
    year suggesting that the presenting
    HPLC preparation is a better and more
    precise method than the previous
    method of using ion exchange
    chromatography.
    Appears in Collections:[保健營養系(所) ] 校內計畫

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